15A Micro-crystal X-ray diffraction

 ★ Tricks of performing single crystal X-ray diffraction at TPS 15A. The document includes the following topics, PLEASE read the document carefully before your beamtime. (Link)

I.General procedures of solving structure

II.Sample preparation at TPS 15A

III.Crystal Handling and Mounting Guidelines

IV.Practical Tips for Identifying a Good Single Crystal

V.How to Start an Experiment?

VI.Large unit cell structure determination is possible: Lysozyme crystal data collection at TPS 15A

VII.How “high order” or “low order” data missing effects the structural refinement

  

★ Please DO fill up the "User's pre-experiment notification of TPS 15A" form one week before your beamtime for your experimental requirements.

    User's pre-experiment notification of TPS 15A

  

★ Please HELP to fill up the "User's feedback of TPS 15A" form after your beamtime to help us to improve our beamline in the future.

    User's feedback of TPS 15A

  

Instrument reservation

 

We appreciate to your coorperation. If you have any questions, please contact the beamline staffs for discussion without hesitate.

Find a Beamline

15A Home

Optical Layout

Endstations

Staff

BL Schedule

Special techniques

Other equipment

For users

Publications

Activity

Useful Links

Orgnisation/association

Files for donwload

Gallery


 Contacts

Endstation

—+886-3-578-0281 Ext. 2151

BL 15A / 15A1 Spokesperson

Wu, Lai-Chin (吳來錦)
wu.lc@nsrrc.org.tw
+886-3-578-0281 Ext. 7343

BL 15A2 Spokesperson

Lee, Jey-Jau (李之釗)
jjlee@nsrrc.org.tw
+886-3-578-0281 Ext. 7116

BL Manager/Local Contact

Grosjean Arnaud (葛阿諾)
a.grosjean@nsrrc.org.tw
+886-3-578-0281 Ext. 7345


Techniques

  • Ambient pressure X-ray photoelectron spectroscopy
  • Single crystal X-ray diffraction
  • Laue diffraction
  • Sub-ns to μs time-resolved structural information
  • Microbeam diffraction
  • Non-ambient technique

Disciplines

  • Medicine and drug discovery
  • Materials science
  • High pressure physics
  • Geoscience
  • Chemistry
  • Functional materials

General Information

  • Source: CUT18
  • Energy Range: 9-35 keV
  • Focused Spot Size: 15A1 ~150 x150 μm² , 15A2 focus to 10 x 10 μm² , Pink-beam with 3 or 5 % bandwidth, optimized at 14 keV
  • Status: Under construction







National Synchrotron Radiation Research Center

101 Hsin-Ann Road, Hsinchu Science Park, Hsinchu, Taiwan 30076

+886-3-578-0281