19A High resolution Powder Diffraction (HRPXRD)
- Structure determination
- Structure refinement/Rietveld refinement
- Cell indexing/Cell refinement
- Phase identification/Phase ratio refinement
- Particle size determination
- In-situ/non-ambient experiments
- Grazing incidence diffraction ( under commission )
Non-ambient sample environments
19A1: X-ray energy range: 16-20 KeV
High resolution PXRD: MYTHEN 18K (Δ2θ: ~ 0.02°)
Ultra-high resolution PXRD: Multi-Crystal Analyzer (Δ2θ: ~ 0.005°)
Available non-ambient sample environments:
1. LN2 cryostream ( 100 K - RT)
2. Hot air gas blower (RT - 1000 °C)
3. LHe Dynaflow cryostat (10 K -150 K)
4. Gas loading system (N2, CO2, Ar, CO, H2)
5. Potentiostat (single cell: Autolab PGSTAT204; multi-cell Biologic VSP3e)
19A2: X-ray energy range: 20-40 KeV
General resolution XRD: XRD 1611 (Δ2θ: ~ 0.04°)
Available non-ambient sample environments:
1. LN2 cryostream ( 100 K - RT)
2. Hot air gas blower (RT - 1000 °C)
3. Potentiostat (single cell: Autolab PGSTAT204; multi-cell Biologic VSP3e)
4. Gas loading system (N2, CO2, Ar, CO, H2)
5. Hot temperature oven (Anton Paar HTK1200N, RT- 1200 °C)
6. High pressure (Diamond anvil cell)