15A Micro-crystal X-ray diffraction

 

15A1    Small molecule single crystal X-ray diffraction

Diffractometer:

Goneometer: Laboratory type, open Eulerian cradle STADIVARI goniometer

Detector: EIGER 2X CdTe 1M

Instrument:

Cryo-system: Cryocool-LN3

Robot for crystal mounting and unmounting

      Techniques:

           1. Small molecule single crystal X-ray diffraction

           2. Photo crystallography with solid state laser

           3. High pressure crystallogarphy with diamond anvil cell (DAC)

Software

Control software: X-area

Data process: X-area, Dials

          

Laboratory type, STADIVARI
open Eulerian cradle goniometer

EIGER 2X CdTe 1M

 

15A2(I)    Advanced micro-crystal X-ray diffraction

                 (Suitable crystal size: < 50 μm)

Diffractometer:

Goneometer: High precision micro-goniometer, MD3-UP

Detector: EIGER 2X CdTe 9M, Dectris

Instrument:

Cryo-system: Cryostream 800

    Techniques:

           1. Pump-probe (time-resolved) crystallography

           2. Photo crystallography with solid state laser

           3. Crystal structure mapping

           4. High pressure crystallogarphy with diamond anvil cell at room

               temperature (Almax plate DAC only)

Software

Control software: MxCuBE

Data process: Dials

 

High precision micro-goniometer,
MD3-UP

EIGER 2X CdTe 9M

 

15A2(II) Motorized stage for extremely condition

Motorized stage to align DAC

Detector: EIGER 2X CdTe 9M, Dectris

Instrument:

Qcryo to cool down a specific DAC

Infrared laser to heating sample in a DAC.

Techniques:

    High pressure crystallogarphy with DAC at room, high and

    low temperature

Find a Beamline

15A Home

Specifications

Endstations

Staff

Current Status

BL Schedule

Special techniques

Other equipment

Files for donwload

Useful Links

Gallery



Techniques

  • Ambient pressure X-ray photoelectron spectroscopy
  • Single crystal X-ray diffraction
  • Laue diffraction
  • Sub-ns to μs time-resolved structural information
  • Microbeam diffraction
  • Non-ambient technique

Disciplines

  • Medicine and drug discovery
  • Materials science
  • High pressure physics
  • Geoscience
  • Chemistry
  • Functional materials

General Information

  • Source: CUT18
  • Energy Range: 9-35 keV
  • Focused Spot Size: 15A1 ~150 x150 μm² , 15A2 focus to 10 x 10 μm² , Pink-beam with 3 or 5 % bandwidth, optimized at 14 keV
  • Status: Under construction







National Synchrotron Radiation Research Center

101 Hsin-Ann Road, Hsinchu Science Park, Hsinchu, Taiwan 30076

+886-3-578-0281